Ball milling: a green technology for the preparation and ...
The ball mill Ball milling is a ... in the presence of DMAP as a catalyst at 200 rpm for 240 hours with an interval of two minutes every 20 minutes of working time. The resulting nanofibrils had a length of several µm and a width in the 1520 nm range. The formation of the ester bonds was monitored by FTIR and the DS measured by ...